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Adding or Editing Synthesis Purification in a Sample

1. In the Purification tab of the Sample (sample name) Synthesis page, click Add, or click Edit next to the item you want to edit. The Add page or Edit page for that item appears.

2. (Purification Type details TBD.)
3. (Protocol details TBD.)
4. (Yield details TBD.)
5. (Design and Methods Description details TBD.)
6. (Technique and Instruments details TBD.)
7. (Finding details TBD.)
8. (Analysis and Conclusion details TBD.)

9. Fill in the information as described in the following table: 

   Section	What to Do
   Purification Type	Fill in the general information about the purification. Select a Purification Type. (TBD: Do we need to provide guidance for choosing interim or final?) Select a Protocol. (TBD: No values show up in this drop-down list for me. Do we need to provide guidance for choosing a value?) Specify the Yield. (TBD: Do we need to provide guidance for specifying a value?)
   Design and Methods	Complete the fields describing techniques and instruments used to derive the data. For details, refer to (link TBD).
   Finding	Click Add to expand the section. Add data findings and supporting documentation relating to the purification. Import as many .csv files as you wish or add derived data manually. For details, refer to (link TBD).
   Analysis and Conclusion	Enter any relevant analyses and conclusions reached by the data.
   Files	Add supporting documentation relating to the purification. Import as many files as you wish. Click Add to expand the section. For

   Add files. For

   details, refer to (link TBD).

10. Click Update.

Defining Purification Techniques and Instruments

When you are adding purification information, fill in the following design, methods, and techniques used.

When you are finished, click Save.

Adding Data Findings to Synthesis Purification 

To add findings to purification information, you can add data directly to Data and Conditions by creating columns and adding data manually or you can import as many .csv files as needed. Information can include laboratory conditions, pH, or temperature. You can add as many files as you wish.

1. Add data values to Data and Conditions.

   1. To import a file of data values

      1. Save the spreadsheet of data values to a csv (comma-separated value) file.

      2. Click Import csv and select and follow the prompts to add the data file to the Findings Info.

      3. The columns and data are added to Data and Conditions.

   2. To add the data values manually

      1. Specify the number of columns and rows for the matrix, and click Update.

      2. Add the data values to the rows.

2. Whether you imported or added information manually, you can preface each data value with one of the following: Maintain the default, equal to (=), or select greater than (>), less than (<), or infinity (approximate).

3. To define a column, click an underlined column heading.
   The Column Definition panel displays.
4. Select a Column Type, Datum or Condition.

5. Select a Column Name or select other and add a new one. You can add up to three cell viability Column Names, including cell viability, cell viability B, and cell viability C. You can further identify the column with the Column Value Type.

   • For Column Type Datum, (Column Name options TBD).

   • For Column Type Condition, (Column Name options TBD). 

6. To further identify a column, select a Column Value Type. Once the column information is saved, the Column Type is shown in parentheses after the Column Name, such as cell viability (mean).

7. Select a Column Value Unit, or select other and add one.

8. If you want the same value to fill all rows in a column, add a Constant Value. For Column Value Type, boolean, enter a Constant Value of 1 for true and 0 for false.

9. Click Save. The system updates the columns. If needed, click Set Column Order to change the order of the column headings in the matrix.

10. Click Save in the Finding section.

Adding Supporting Documents to a Sample

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