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Adding or Editing Synthesis Materials in a Sample

  1. Display the Add or Edit page for synthesis material of a sample, as described in (link TBD).
  2. In the Materials tab of the Sample (sample name) Synthesis page, on the Materials tab, click Add, or click Edit next to the item you want to edit, as described in (link TBD). The Add page or Edit page for that item appears.
  3. Select a protocol and provide a description. (TBD: What guidance can we provide here for specifying a protocol & description?)
  4. In the Materials panel, click Add and fill in the following information.

    CompleteHow to
    Material Type*

    Select the type of material comprising this nanomaterial (required).

    Chemical Name*Enter the chemical name given to the atomic or molecular structure that composes the center of the nanoparticle (required).
    PubChem Data Source

    Select one of the three PubChem data sources: Compound, Substance, or BioAssay. The database is located here:

    http://pubchem.ncbi.nlm.nih.gov/

    . (TBD: On Dev, the Materials panel doesn't have PubChem ID field. Is that intentional?)

    Amount/Amount Unit

    Include Page
    Amount unit
    Amount unit

    Molecular Formula Type

    Include Page
    Molecular formula type
    Molecular formula type

    Molecular FormulaEnter the chemical formula of the nanoparticle.
    Supplier NameSelect the supplier name. (TBD: What guidance can we provide here for selecting the supplier name?) 
    LotSpecify the lot. (TBD: What guidance can we provide here for specifying the lot?) 
    Material DescriptionEnter a description for the composing element.
    Inherent Functions

    Next to Inherent Functions, click Add to expand the panel. An inherent function is the characteristic behavior of a sample that results from the chemical and physical composition and properties of the entity. For details, refer to (link TBD).

  5. Click Save Material Element
  6. Add files. For details, refer to (link TBD).
  7. If editing the synthesis material, click Update

Adding or Editing Synthesis Functionalization in a Sample

  1. Display the Add or Edit page for synthesis functionalization of a sample, as described in (link TBD).
  2. In the Functionalization tab of the Sample (sample name) Synthesis page, on the Functionalization tab, click Add, or click Edit next to the item you want to edit, as described in (link TBD). The Add page or Edit page for that item appears.
  3. Select a protocol and provide a description. (TBD: What guidance can we provide here for specifying a protocol & description?)
  4. In the Functionalization Materials panel, click Add and fill in the following information: 

    PubChem data source

    (TBD: This panel is similar to composition, but Dev GUI On Dev, the Materials panel doesn't have PubChem ID field. Is that intentional?)

    CompleteHow to
    Functionalization Type*

    Select the type of material comprising this nanomaterial (required).

    Chemical Name*Enter the chemical name given to the atomic or molecular structure that composes the center of the nanoparticle (required).
    PubChem Data Source/PubChem ID

    Select one of the three PubChem data sources: Compound, Substance, or BioAssay. The database is located here:

    http://pubchem.ncbi.nlm.nih.gov/

    Include Page
    PubChem data source
    Amount/Amount Unit

    Include Page
    Amount unit
    Amount unit

    Molecular Formula Type

    Include Page
    Molecular formula type
    Molecular formula type

    Molecular FormulaEnter the chemical formula of the nanoparticle.
    Functionalization DescriptionEnter a description for the composing element.
    Inherent Functions

    Next to Inherent Functions, click Add to expand the panel. An inherent function is the characteristic behavior of a sample that results from the chemical and physical composition and properties of the entity. For details, refer to (link TBD).

  5. Click Save Functionalization Element
  6. Add files. For details, refer to (link TBD).
  7. If editing the synthesis functionalization, click Update.

Adding or Editing Synthesis Purification in a Sample

  1. Display the Add or Edit page for synthesis purification of a sampleIn the Sample (sample name) Synthesis page, on the Purification tab, click Add, or click Edit next to the item you want to edit, as described in (link TBD). The Add page or Edit page for that item appears.
  2. Fill in the information as described in the following table: 

    PanelWhat to Do
    Purification Type

    Fill in the general information about the purification.

    • Select a Purification Type. (TBD: What guidance can we provide here for choosing interim or final?)

    • Select a Protocol. (TBD: In the Dev tier, no values show up in this drop-down list for me. Do we need to provide guidance for choosing a value?)

    • Specify the Yield. (TBD: What guidance can we provide here for specifying a value?)

    Design and Methods

    Fill in the design and methods information about the purification.

    • In the Design and Methods Description field, enter a description for the purification design and methods.

      Info
      titleAdding extra lines

      If you include an extra line between text in the Design and Methods Description, the line separation is preserved when you save or update the purification information.

    • Next to Technique and Instruments, click Add to expand the panel. For details on specifying techniques and instruments used to derive the data, refer to (link TBD).
    Finding

    Click Add to expand the panel. Add data findings and supporting documentation relating to the purification. Import as many .csv files as you wish or add derived data manually. For details, refer to (link TBD).

    Analysis and ConclusionEnter any relevant analyses and conclusions reached by the data. 
    Files

    Click Add to expand the panel. (TBD: On the Dev tier, nothing happens when I click Add in the purification Files panel.) Add supporting documentation relating to the purification. Import as many files as you wish. For details, refer to (link TBD).

  3. If editing the synthesis purification, click Update.

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